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Download e-book for iPad: Amino Acids and Peptides (SPR Amino Acids, Peptides by J. S. Davies

By J. S. Davies

ISBN-10: 0851862241

ISBN-13: 9780851862248

Professional Periodical experiences supply systematic and exact evaluate assurance of growth within the significant parts of chemical learn. Written through specialists of their expert fields the sequence creates a special provider for the lively study chemist, providing commonplace severe in-depth money owed of development specifically components of chemistry.

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Additional info for Amino Acids and Peptides (SPR Amino Acids, Peptides (RSC))vol. 24

Example text

The C33- CB8portion of the calyculins is a (2R,3R,4R)-2,3dihydroxy-4-dimethylamino-5-methoxypentanoic acid residue, and is thus closely related to the statines. "6 &Amino acids and higher homologues are generally accessible through standard organic synthesis methodology, as opposed to the particular methods that are recognizable to the protein amino acid chemist. 299A lactone almost identical with the above-mentioned lactone (59; NHCPh3 in place of OH) has been prepared from L-phenylalanine for synthetic studies in this area, through the transformation C02Me+-COCH?

179). 378 Hydrogen-bonding pairing (65) involving N-succinoyl L - p r ~ l i n e ,is~ ~ ~ revealed by the 32-fold alteration of the amide cis:trans ratio after presentation of the hydrogen-bonding partner. 49). 389The binding constants are two orders of magnitude greater than those involving simple electron acceptors such as methylviologen. 392 A similar, and equally important inference,393has been drawn, based on comparisons of water-to-vapour and water-to-cyclohexane distribution coefficients for N-acetylpyrrolidine and N-butylacetamide.

R. r. r. r. r. measurements have been reported for methyl (S)-( + )-mandelate esters of N,N-dimethylamino confirmed with interpretation of corresponding data for p-nitroanilides of these amino acids in chiral solvents. A modified Mosher method has been developed further, in which shift values for protons in N-(2-methoxy-2-phenyl-2-trifluoromethyl)acetyl derivatives of amines and amino acid esters are determined. 1 mg of an amino acid. s. '^^ Glutamic and aspartic acids, alanine, proline, and lysine from different origins show wide variations.

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Amino Acids and Peptides (SPR Amino Acids, Peptides (RSC))vol. 24 by J. S. Davies


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